Quarterly Journal of the Chemical Society of London, Volume 8, Pages 1365-2022 |
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Page 1571
... chloride yields a mixture of phenyltolylmethanes , and not bibenzyl as previously reported . Similar treatment of p - xylene gives 4 - tolyl - 2,5 - xylylmethane and 2 - chloro - p - xylene , and mesitylene yields 2 - chloromesitylene ...
... chloride yields a mixture of phenyltolylmethanes , and not bibenzyl as previously reported . Similar treatment of p - xylene gives 4 - tolyl - 2,5 - xylylmethane and 2 - chloro - p - xylene , and mesitylene yields 2 - chloromesitylene ...
Page 1593
... chloride ( mesitoyl chloride ) and the 2,4,6 - triphenylbenzoyl chloride . The mesitoyl chloride - aluminium chloride complex reacts similarly . The n.m.r. spectra shows the formation of the tropylium ion but no aldehydic signal ...
... chloride ( mesitoyl chloride ) and the 2,4,6 - triphenylbenzoyl chloride . The mesitoyl chloride - aluminium chloride complex reacts similarly . The n.m.r. spectra shows the formation of the tropylium ion but no aldehydic signal ...
Page 1596
... chloride ( 7.8 g . ) and aluminium chloride ( 13.4 g . ) in methylene chloride ( 100 ml . ) at -20 ° . The mixture was worked up as for ( XIa ) to give the product ( 22 % yield , 2.9 g . ) , b.p. 91-95 ° ( 10 mm . ) , M + 134-0712 , C ...
... chloride ( 7.8 g . ) and aluminium chloride ( 13.4 g . ) in methylene chloride ( 100 ml . ) at -20 ° . The mixture was worked up as for ( XIa ) to give the product ( 22 % yield , 2.9 g . ) , b.p. 91-95 ° ( 10 mm . ) , M + 134-0712 , C ...
Contents
Organic chemistry | 1365 |
Substituted oxindoles Part IV 3Alkylation of 1methylindol23Hone 1methyloxindole | 1375 |
Contents iii | 1377 |
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1-phosphate absorption acetic acid acetic anhydride acetone added adduct alcohol alkyl Amer amine anhydride anhydrous aqueous aromatic atom benzene bromide Calc carbonyl CH₂ Chem chloride chloroform chromatography cm.¹ compound conj cooled crystallised cyclohexanone cyclopentadiene derivatives deuterium diene dimethyl dimethylbutadiene distilled dried eluted ester ethanol ethyl acetate evaporated extracted with ether filtered Found fraction gave give heated under reflux hydrazine hydride hydrochloric hydrogen carbonate hydrolysis hydroxide i.r. spectrum iodide isolated isomer ketone light petroleum mass spectrum methyl methylene mixed m.p. mmHg mole n.m.r. spectrum needles nitrogen obtained olefin oxalylindene oxide petroleum petroleum b.p. phosphate potassium prepared protons pyridine quinone reaction rearrangement reduced pressure requires residue ring room temperature showed silica gel sodium sodium hydroxide solid solution solvent spectra structure substituent Table washed yellow yield