Quarterly Journal of the Chemical Society of London, Volume 8, Pages 1365-2022 |
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Page 1786
... hydroxide ( 0.01 mol ) in water ( 9 ml ) . As soon as the blue colour appeared , additional sodium hydroxide solution ( 0.01 mol ) was added . The blue colour faded and the bromocresol was recovered in 70 % yield . When the bromocresol ...
... hydroxide ( 0.01 mol ) in water ( 9 ml ) . As soon as the blue colour appeared , additional sodium hydroxide solution ( 0.01 mol ) was added . The blue colour faded and the bromocresol was recovered in 70 % yield . When the bromocresol ...
Page 1857
... hydroxide at room temperature has been confirmed , and shown to be an autoxidation reaction . Autoxidation of 9 ( 10 ) -hydroxy10 ( 9 ). THE reaction of 9 ( 10 ) -hydroxy - 10 ( 9 ) -oxo - octadecanoic acid ( 1 ) with alkali metal ...
... hydroxide at room temperature has been confirmed , and shown to be an autoxidation reaction . Autoxidation of 9 ( 10 ) -hydroxy10 ( 9 ). THE reaction of 9 ( 10 ) -hydroxy - 10 ( 9 ) -oxo - octadecanoic acid ( 1 ) with alkali metal ...
Page 1894
... hydroxide ( 300 ml . ) was distilled . The volume was kept approximately constant by addition of water . The distil- late ( 300 ml . ) was acidified with 2N - hydrochloric acid ( 45 ml . ) , and the solution was kept at 80 ° for 1 hr ...
... hydroxide ( 300 ml . ) was distilled . The volume was kept approximately constant by addition of water . The distil- late ( 300 ml . ) was acidified with 2N - hydrochloric acid ( 45 ml . ) , and the solution was kept at 80 ° for 1 hr ...
Contents
Organic chemistry | 1365 |
Substituted oxindoles Part IV 3Alkylation of 1methylindol23Hone 1methyloxindole | 1375 |
Contents iii | 1377 |
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1-phosphate absorption acetic acid acetic anhydride acetone added adduct alcohol alkyl Amer amine anhydride anhydrous aqueous aromatic atom benzene bromide Calc carbonyl CH₂ Chem chloride chloroform chromatography cm.¹ compound conj cooled crystallised cyclohexanone cyclopentadiene derivatives deuterium diene dimethyl dimethylbutadiene distilled dried eluted ester ethanol ethyl acetate evaporated extracted with ether filtered Found fraction gave give heated under reflux hydrazine hydride hydrochloric hydrogen carbonate hydrolysis hydroxide i.r. spectrum iodide isolated isomer ketone light petroleum mass spectrum methyl methylene mixed m.p. mmHg mole n.m.r. spectrum needles nitrogen obtained olefin oxalylindene oxide petroleum petroleum b.p. phosphate potassium prepared protons pyridine quinone reaction rearrangement reduced pressure requires residue ring room temperature showed silica gel sodium sodium hydroxide solid solution solvent spectra structure substituent Table washed yellow yield