Journal of the Chemical SocietyThe Society., 1960 |
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Page 228
... Hydrochloride . - Amino - oxyacetic acid half - hydrochloride ( 1 g . ) was suspended in dry ether and treated with dry hydrogen chloride until the solution was saturated . The hydrochloride was collected and washed with dry ether and ...
... Hydrochloride . - Amino - oxyacetic acid half - hydrochloride ( 1 g . ) was suspended in dry ether and treated with dry hydrogen chloride until the solution was saturated . The hydrochloride was collected and washed with dry ether and ...
Page 234
... hydrochloride as white plates ( 1.4 g . ) , m . p . 148-149 ° ( lit. , 35 m . p . 149 ° ) . Amino - oxyethane hydrochloride similarly prepared , formed plates ( from ethyl acetate- ethanol ) , m . p . 130—132 ° ( lit. , 36 m . p . 128 ...
... hydrochloride as white plates ( 1.4 g . ) , m . p . 148-149 ° ( lit. , 35 m . p . 149 ° ) . Amino - oxyethane hydrochloride similarly prepared , formed plates ( from ethyl acetate- ethanol ) , m . p . 130—132 ° ( lit. , 36 m . p . 128 ...
Page 235
... hydrochloride was obtained as leaflets , m . p . 143–144 ° ( Found : C , 59-1 ; H , 11-4 ; N , 6-0 . C11H26ONCI requires C , 59-0 ; H , 11-7 ; N , 6 · 2 % ) . 2 - Amino - oxyundecane hydrochloride crystallised similarly ( m . p . 145 ...
... hydrochloride was obtained as leaflets , m . p . 143–144 ° ( Found : C , 59-1 ; H , 11-4 ; N , 6-0 . C11H26ONCI requires C , 59-0 ; H , 11-7 ; N , 6 · 2 % ) . 2 - Amino - oxyundecane hydrochloride crystallised similarly ( m . p . 145 ...
Contents
NO PAGE | 6 |
Tautomerism of Nheteroaromatic aldoximes | 22 |
Nucleophilic displacements in organic sulphites Part VI Comparison of | 37 |
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Common terms and phrases
acetic acid alcohol alkaline Amax Amer amylose anhydride aniline aqueous sodium ation atom bands benzene benzoic acid benzoyl peroxide boiled bond boron bromide butyl Calc calculated carbon tetrachloride CH₂ Chem chloride chlorobenzene chloroform chromatography complex component compounds concentration constants cooled crystallised cyclic sulphate cyclohexane decomposition derivatives dilute distilled dried equation ester ethanol ether ethyl acetate evaporated EXPERIMENTAL extracted Fèvre filtered filtrate formed Found fraction gave H₂O heated hydrochloride hydrogen hydrogen chloride hydrolysis imino-ether infrared iodide ions isolated k₁ ketone m. p. and mixed method mixed m. p. mixture mole molecular molecules needles NH₂ nitration nitrogen obtained oxide peroxide phenol picrate potassium precipitate prepared pyridine reaction reduced reflux removed requires residue room temperature sample sodium hydroxide solution solvent spectra spectrum Table thiocyanate thiocyanogen transition values vanadium(IV wavelengths yield Z-enzyme