Quarterly Journal of the Chemical Society of London, Volume 1 |
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Page 194
... ether ) ( Found : C , 54 · 0 ; H , 7-1 ; N , 11 · 4 . C11H17CIN2O2 requires C , 54 · 0 ; H , 7 · 0 ; N , 11 · 4 % ) . 3 - Carbamoyl - 1,4 - dihydro - 1 - propoxymethylpyridine.- Di- ethyl ether ( 500 c.c. ) was added to a solution of 3 ...
... ether ) ( Found : C , 54 · 0 ; H , 7-1 ; N , 11 · 4 . C11H17CIN2O2 requires C , 54 · 0 ; H , 7 · 0 ; N , 11 · 4 % ) . 3 - Carbamoyl - 1,4 - dihydro - 1 - propoxymethylpyridine.- Di- ethyl ether ( 500 c.c. ) was added to a solution of 3 ...
Page 286
... ether ( 40 ml . ) and ethanol ( 10 ml . ) , and ethyl n - butylcyanoacetate ( 2 · 7 ml . ) was added . To the solution of the sodio - ester thus formed , a suspension of triphenyl- phosphinegold ( 1 ) chloride ( 3 g . ) in ether ( 20 ml ...
... ether ( 40 ml . ) and ethanol ( 10 ml . ) , and ethyl n - butylcyanoacetate ( 2 · 7 ml . ) was added . To the solution of the sodio - ester thus formed , a suspension of triphenyl- phosphinegold ( 1 ) chloride ( 3 g . ) in ether ( 20 ml ...
Page 422
... ether ) . The ether solution was dried and the ether re- moved . The residual oil had an i.r. spectrum identical with that of 1 - chloro - 3 - hydroxyacetone synthesised indepen- dently . The product crystallised in a few days at 0 ...
... ether ) . The ether solution was dried and the ether re- moved . The residual oil had an i.r. spectrum identical with that of 1 - chloro - 3 - hydroxyacetone synthesised indepen- dently . The product crystallised in a few days at 0 ...
Contents
Physical organic chemistry | 1 |
Aromatic reactivity Part XXXVIII Protodesilylation of 12dihydrobenzocyclobutene indan and tetralin | 12 |
Aromatic reactivity Part XL Additional substituent effects in protodetrimethylsilylation | 21 |
Copyright | |
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absorption acetic acid activation added addition alcohol Amer analysis angles appears aqueous atom base benzene bond bromide calculated carbon carbon tetrachloride Chem chemical chloride compared complex compounds concentration conformation constants containing corresponding coupling derived described determined DISCUSSION effect electron energy equation esters ethanol ether expected experimental experiments factor Figure followed formation formed further gave give given hydrogen hydrolysis increase indicate initial intermediate involving kinetic less measured mechanism method methyl mixing mixture mole molecular molecule nitration observed obtained occurs organic oxidation oxygen peaks peroxide Phys plot position possible prepared present pressure proton radical rate constants ratio reaction reactivity reduced relative reported requires resonance respectively ring salts shifts showed shown similar sodium solution solvent spectra spectrum structure studied substituent suggested Table temperature values yield