Quarterly Journal of the Chemical Society of London |
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Results 1-3 of 81
Page 1858
... lithium aluminium hydride ( 2.0 g . ) in dioxan ( 100 c.c. ) was refluxed for 1 hr . Addition of water and distillation of the product gave 1 - vinylcyclohexanol ( 3.0 g . ) , b . p . 62—64 ° / 11 mm . , n 1 · 4758 ( Nazarov et al ...
... lithium aluminium hydride ( 2.0 g . ) in dioxan ( 100 c.c. ) was refluxed for 1 hr . Addition of water and distillation of the product gave 1 - vinylcyclohexanol ( 3.0 g . ) , b . p . 62—64 ° / 11 mm . , n 1 · 4758 ( Nazarov et al ...
Page 1859
... lithium aluminium hydride ( 2.85 g . ) , and the mixture was heated under reflux for 4 hr . Isolation of the product gave pent - 2 - en - 4 - yn - 1 - ol ( 1.7 g . ) , b . p . 61 ° / 10 mm . , no 1 · 4970 ( Haynes et al . , loc . cit ...
... lithium aluminium hydride ( 2.85 g . ) , and the mixture was heated under reflux for 4 hr . Isolation of the product gave pent - 2 - en - 4 - yn - 1 - ol ( 1.7 g . ) , b . p . 61 ° / 10 mm . , no 1 · 4970 ( Haynes et al . , loc . cit ...
Page 2147
... Lithium Aluminium Hydride . The toluene - p - sulphonate ( 10 g . ) in dry tetrahydrofuran ( 50 c.c. ) was added gradually with stirring to lithium aluminium hydride ( 4.5 g . ) in tetrahydrofuran ( 200 c.c. ) The mixture was refluxed ...
... Lithium Aluminium Hydride . The toluene - p - sulphonate ( 10 g . ) in dry tetrahydrofuran ( 50 c.c. ) was added gradually with stirring to lithium aluminium hydride ( 4.5 g . ) in tetrahydrofuran ( 200 c.c. ) The mixture was refluxed ...
Contents
C52j | 1174 |
Lanthanon Complexes with Ethylenediaminetetraacetic Acid Part IV | 1181 |
The Bodroux Reaction | 1188 |
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absorption acetic acid acetic anhydride acetone acetyl ajmaline alcohol alkaline alkyl Amer amine ation atoms B.Sc benzene boiling bond bromine Calc carbon CH₂ Chem Chemistry chloroform colourless complex compound concentration crystallised D.Sc decomp decomposition derivatives dilute dioxan dissolved distilled dried eluted ester ethanol ether ethyl acetate evaporated extracted filtered formation formed Found fraction gave give m. p. heated hydrochloric acid hydrogen chloride hydrolysis iodide isolated ketone light petroleum b. p. lithium aluminium hydride m. p. and mixed method methyl mixed m. p. mixture molecule obtained oxide oxygen perchlorate Ph.D phenol piperidine potassium hydroxide precipitate prepared prisms pyridine reaction reagent reduction refluxed Reprint Order requires residue room temperature salt separated sodium hydroxide solid solution solvent spectra sulphate sulphuric acid Table triethylamine vacuo values washed yellow needles yield